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文獻名：Application of LF-NMR to the characterization of camellia oil-loaded pickering emulsion fabricated by soy protein isolate

 

 

作者： Chen Wang, Xin Wang, Caiyun Liu, Conghui Liu

School of Medical Instrument and Food Engineering, University of Shanghai for Science and Technology, Shanghai, 200093, China

 

摘要：In this study, the camellia oil-loaded Pickering emulsion stabilized by soybean protein isolate (SPI) was selected, and low-field nuclear magnetic resonance were adopted to characterize the emulsion transformation process besides conventional characterization index. Results showed that the T₂ distribution of SPI dispersion only showed one hydrogen pool, and T_cur, T_2W and T₂ all decreased with the increase of SPI concentration, indicating faster decay and lower proton mobility, which was companied by increasing particle diameter. The addition of NaCl and heating (95 °C, 15 min) can speed up the relaxation decay, increase the surface hydrophobicity and reduce the nanoparticle diameter. As for the emulsion, three hydrogen populations were observed on T₂ distribution. Based on the correlation results, the hydrogen pools were successfully attributed to oil and water phase, respectively. Meanwhile, with the increase of oil volume fraction (0.1–0.6), the T_cur and T_2W tended to decrease, the absorbed protein percentage (AP%) and the shear viscosity tended to increase, while the droplet diameter only increased significantly when ? was below 0.3. Lastly, the T₂ distribution of the oleogel showed two hydrogen populations, and the population (T₂₂) could be interpreted as the mobility of protons in oil molecules, which accounted for more than 95% of the total signal. Although the elastic properties of oleogel became weaker with the increase of ?, the T_cur and T_2W were relatively stable. However, it was significantly distinctive from that of SPI dispersion and emulsion. In summary, LF-NMR could be used for the rapid characterization of emulsion.

 

關鍵詞：LF-NMR；Emulsion；Characterization；Camellia oil；Soybean protein isolate